New nano-based filter for infrared light promises cheap, robust spectrometers

Lisa Lock
scientific editor

Andrew Zinin
lead editor

A new filter for infrared light could see scanning and screening technology tumble in price and size. Built on nanotechnology, the new heat-tunable filter promises hand-held, robust technology to replace current desktop infrared spectroscopy setups that are bulky, heavy and cost from $10,000 up to more than $100,000.
Because the new technology is built on silicon technology, its manufacture can be scaled, with the potential to push costs down below $1 per filter, its developers said.
"The mid-infrared is ripe for technological development," said Professor Kenneth Crozier, Deputy Director of the ARC Center of Excellence for Transformative Meta-Optics (TMOS), who leads the research group.
"There are high-performance systems available, but they are expensive. This smaller, lighter, low-power technology could open up a lot of applications; for example, field testing of agricultural products, such as milk and olive oil, and screening and sorting of recycled materials."
The research is in Laser and Photonics Reviews.
Many materials can be easily identified from the way they absorb different parts of the infrared spectrum, so infrared spectroscopy is useful for monitoring contaminants, for example in industrial processes.
Spectroscopy relies on spreading the light source into a spectrum, which is conventionally done with a grating or prism to spread the infrared light: Different parts of the spectrum are sent into the sample by tilting the grating back and forth.
For robustness, the TMOS team instead opted for a non-moving component to select specific parts of the infrared spectrum, in the form of a band-pass filter. Drawing on other research within TMOS that had used heating to vary component behavior, they devised a filter with temperature-dependent band-pass wavelength.
This is made possible by making the filter from silicon, whose refractive index shifts smoothly with temperature.
"The great thing about it is that it is very stable and reversible," said Ben Russell, Ph.D. student in TMOS.
To generate bandpass behavior from the silicon, the team used a metasurface, a layer of silicon approximately 1.5 microns thick with an array of nanoscale features carved into it, sitting on a layer of sapphire (Al2O3) 470 microns thick.
Initially Russell modeled the dimensions of the metasurface, coming up with two possible solutions: parallel grooves 1,002 nm deep, spaced 1,683 nm apart, and crossed grooves, 1,060 nm deep and 1,684 nm apart. While the parallel grooves gave better spectral properties, they were sensitive to the polarization of the light, whereas the two-dimensional, crossed pattern was not.
Russell then created prototypes of both by carefully etching the pattern into an off-the-shelf silicon-on-sapphire wafer鈥攚hich needed a few repeats, as he initially underestimated the etching rate.
Sure enough, the finished prototype behaved as modeled, displaying a linear wavelength shift of 80 nanometers, across the standard operating temperatures from 25掳C to 420掳C. More extreme heating and cooling to cryogenic temperatures extended this to 140 nm鈥攁lthough these extremes are unlikely to be of practical use in the future.
With stable temperature tuning achieved, the team tested the spectroscopic capabilities of the filter on a number of everyday items, for example, successfully measuring polymide tape and a zinc selenide window.
They were also pleased to be able to easily distinguish between two clear, recyclable plastics of different composition, LDPE and PET.
"Folks in environmental monitoring, agriculture, and industrial process control and safety already understand the utility of portable infrared spectroscopy tools. The proliferation of compact, inexpensive, and reliable spectrometers will be a boon, and our results bring us another step closer," state the researchers.
More information: Benjamin J. Russell et al, Thermo-Optically Tunable Mid-Infrared Bandpass Filters Comprising Ultra鈥怲hin Silicon-on-Sapphire Metasurfaces, Laser & Photonics Reviews (2025).
Provided by RC Centre of Excellence for Transformative Meta-Optical Systems (TMOS)